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Number of results: 14
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Abstract

Noise diagnostics has been performed on the cold field-emission cathode in high-vacuum. The tested cold field-emission cathode, based on tungsten wire with ultra-sharp tip coated by epoxy was designed to meet the requirements of transmission electron microscopy, which uses a small and stable source of electrons. Current fluctuations are reduced by improving the structure and fabrication technology. Noise was measured both in time and frequency domains, which gives information about current fluctuations and also about charge transport. Mutual correlation between the noise spectral density, extractor voltage and beam brightness was analyzed.

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Authors and Affiliations

Alexandr Knápek
Lubomír Grmela
Josef Šikula
Ondřej Šik
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Abstract

Samples of CdTe single crystals which are used as radiation detectors were periodically measured during a long time interval with different values of an applied voltage. The samples were also periodically exposed during long time periods to high temperatures of 390 K and to rapid changes of temperature from 300 K to 390 K. After 1.5 years of measurements we observed ageing of the samples which resulted in deterioration of their transport characteristics. The resistance of the samples increased significantly and current-voltage characteristics were unstable in time. Noise spectroscopy showed that low frequency noise can be used for detection of CdTe sample ageing as its spectral density increases significantly comparing to the 1/f noise of a high quality sample

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Authors and Affiliations

Lubomír Grmela
Ondřej Šik
Alexey Andreev
Josef Sikula
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Abstract

In this study, Al 2024-T3 alloy plates were joined by using friction stir welding. Welding was performed at a rotational speed of 930, 1450, 2280 rpm and a welding feed rate of 180 mm min −1. The welded samples were analyzed at the microstructural level. Moreover, both bending fatigue tests and tensile tests were performed on samples. At the end of the microstructural examination of the samples welded at the rotational speed of 930 rpm and the welding feed rate of 180 mm min −1, the formation of tunnel defects was observed. The highest fatigue life was obtained at 2280 rpm and 180 mm min −1. The lowest fatigue life was obtained at 930 rpm and 180 mm min −1. The highest ultimate tensile stress was obtained at 2280 rpm/180 mm min –1 sample, which shows about a 12% reduction relative to the base material. The lowest ultimate tensile stress was obtained at 930 rpm/180 mm min –1 sample. The ultimate tensile stress value of the 930 rpm/180 mm min –1 sample decreased by approximately 25%.
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Authors and Affiliations

A. Şık
1
ORCID: ORCID
A. Özer
2
ORCID: ORCID

  1. Gazi University, Faculty of Architecture, Department of Industrial Design, 06570 Maltepe, Ankara, Turkey
  2. Gazi University, Technical Sciences Vocational School, 06374 Ostim, Yenimahalle, Ankara, Turkey
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Abstract

Direct energy deposition (DED) is a three-dimensional (3D) deposition technique that uses metallic powder; it is a multi-bead, multi-layered deposition technique. This study investigates the dependence of the defects of the 3D deposition and the process parameters of the DED technique as well as deposition characteristics and the hardness properties of the deposited material. In this study, high-thermal-conductivity steel (HTCS-150) was deposited onto a JIS SKD61 substrate. In single bead deposition experiments, the height and width of the single bead became bigger with increasing the laser power. The powder feeding rate affected only the height, which increased as the powder feeding rate rose. The scanning speed inversely affected the height, unlike the powder feeding rate. The multi-layered deposition was characterized by pores, a lack of fusion, pores formed by evaporated gas, and pores formed by non-molten metal inside the deposited material. The porosity was quantitatively measured in cross-sections of the depositions, revealing that the lack of fusion tended to increase as the laser power decreased; however, the powder feeding rate and overlap width increased. The pores formed by evaporated gas and non-molten metal tended to increase with rising the laser power and powder feeding rate; however, the overlap width decreased. Finally, measurement of the hardness of the deposited material at 25℃, 300℃, and 600℃ revealed that it had a higher hardness than the conventional annealed SKD61.

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Authors and Affiliations

Jong-Youn Son
Gwang-Yong Shin
Ki-Yong Lee
Hi-Seak Yoon
Do-Sik Shim
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Abstract

In the electropolishing process, the polishing quality of the metal surface varies according to the contamination of the electrolyte. In this study, the electrolyte was evaluated according to the usage time, and the effect of each factor on electropolishing was investigated. As the electrolyte is contaminated, the concentration of metal ions in the electrolyte increases and the ion conductivity decreases. In addition, the pH and specific gravity of the electrolyte increase due to the metal sludge formed as the metal ion concentration increases. When the electrolyte usage time was more than 5 days, many scratches remained on the surface of 316L stainless steel, and relatively high surface roughness was measured. The surface roughness improvement rate compared to the initial specimen was 30% for the unused electrolyte, 26% on the 3rd day, 19% on the 5th day, and 17.5% on the 13th day. Since the low current density due to electrolyte contamination causes a decrease in polishing efficiency, initial scratches on the metal surface still exist on the polished surface. Therefore, it is necessary to manage the electrolyte to maintain the quality of electropolishing.
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Authors and Affiliations

Woo-Chul Jung
1
ORCID: ORCID
Hyunseok Yang
1
ORCID: ORCID
Seon-Jin Choi
2
ORCID: ORCID
Man-Sik Kong
1
ORCID: ORCID

  1. Advanced Material & Processing Center (Institute for Advanced Engineering, Yongin, Korea)
  2. Division of Materials Science and Engineering, Hanyang University, Seoul, South Korea
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Abstract

MoO3 thick film was manufactured by using a thermal spray process (Atmospheric Plasma Spray, or APS) and its microstructure, phase composition and properties of the coating layer were investigated. Initial powder feedstock was composed of an orthorhombic α-MoO3 phase, and the average powder particle size was 6.7 μm. As a result of the APS coating process, a MoO3 coating layer with a thickness of about 90 μm was obtained. Phase transformation occurred during the process, and the coating layer consisted of not only α-MoO3 but also β-MoO3, MoO2. Phase transformation could be due to the rapid cooling that occurred during the process. The properties of the coating layer were evaluated using a nano indentation test. Hardness and reduced modulus were obtained as 0.47 GPa and 1.4 GPa, respectively. Based on the above results, the possibility of manufacturing a MoO3 thick coating layer using thermal spray is presented.
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Authors and Affiliations

Yu-Jin Hwang
1
ORCID: ORCID
Kyu-Sik Kim
1 2
ORCID: ORCID
Jae-Sung Park
3
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon, Korea
  2. Agency for Defense Development, Daejeon, Korea
  3. LT Metal, Seoul, Korea
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Abstract

Co-Cr-Mo based sheet I-WP lattice was fabricated via laser powder bed fusion. The effect of microstructure and the I-WP shape on compressive mechanical response was investigated. Results of compression test showed that yield strength of the sheet I-WP was 176.3 MPa and that of bulk Co-Cr-Mo (reference material) was 810.4 MPa. By applying Gibson-Ashby analytical model, the yield strength of the lattice was reversely estimated from that of the bulk specimen. The calculated strength of the lattice obtained was 150.7 MPa. The shape of deformed lattice showed collective failure mode, and its microstructure showed that strain-induced martensitic transformation occurred in the overall lattice. The deformation behavior of additively manufactured sheet I-WP lattice was also discussed.
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Authors and Affiliations

So-Yeon Park
1
ORCID: ORCID
Kyu-Sik Kim
2
ORCID: ORCID
Bandar Almangour
3
ORCID: ORCID
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon, Korea
  2. Agency for Defense Development, Daejeon, Korea
  3. Interdisciplinary Research Center for Intelligent Manufacturing & Robotics, King Fahd University of Petroleum & Minerals, Dhahran, Saudi Arabi
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Abstract

Intermetallic γ-TiAl alloy has excellent properties at high temperatures and is thus attracting attention as a substitute for nickel-based superalloy parts for turbine engines. However, γ-TiAl alloy is reported to be a difficult material to be machined due to its low ductility at room temperature, tensile strength, and thermal conductivity. In this study, a system capable of measuring thrust force (Tf) and torque (Tc) during the drilling process was constructed, and drilling processability according to the heat treated microstructure of γ-TiAl alloy was compared. As a result, it was confirmed that the thrust and torque of the γ-TiAl alloy having a microstructure in which the grains were refined by the heat treatment process was relatively low and rapidly stabilized, which is advantageous for drilling.
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Bibliography

[1] M. Rahman, Y.S. Wong, A.R. Zareena, Machinability of titanium alloys, JSME Series C 46 (1), 107-115 (2003).
[2] A. Beranoagirre, G. Urbikain, A. Calleja, L. Lacalle, Drilling Process in γ-TiAl Intermetallic Alloys, Materials (Basel) 2018 Dec; 11 (12): 2379. Published online 2018 Nov 26. DOI: https://doi.org/10.3390/ma11122379
[3] S . Castellanos, A. Cavaleiro, Machinability of titanium aluminides: a review, Proceedings of the Institution of Mechanical Engineers 233, 3, 426-451. DOI: https://doi.org/10.1177/1464420718809386
[4] M. Thomas, M.P. Bacos. Processing and Characterization of TiAlbased Alloys: Towards an Industrial Scale. AerospaceLab 3, 1-11 (2011). hal-01183638
[5] J.H. Kim, J.K. Kim, S.W. Kim, Y.H Park, S.E. Kim, Effect of Microstructure Control on the Mechanical Properties of Hot Worked TiAl Alloy, Korean J. Met. Mater. 58, 7, 459-465 (2020). DOI: https://doi.org/10.3365/KJMM.2020.58.7.459
[6] S . Bhowmick, A. Alpas, Minimum quantity lubrication drilling of aluminium – silicon alloys in water using diamond-like carbon coated drills, International Journal of Machine Tools & Manufacture 48, 1429-1443 (2008).
[7] J.N. Wang, J. Yang, Q. Xia, Y. Wang, On the grain size refinement of TiAl alloys by cyclic heat treatment, Materials Science and Engineering A 329-331, 118-123. DOI: https://doi.org/10.1016/S0921-5093(01)01543-X
[8] P.C. Priarone, S. Rizzuti, G. Rotella, Tool wear and surface quality in milling of a gamma-TiAl intermetallic. International Journal of Advanced Manufacturing Technology 61, 25-33 (2012). DOI: https://doi.org/10.1007/s00170-011-3691-x
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Authors and Affiliations

Hyunseok Yang
1 2
ORCID: ORCID
Woo-Chul Jung
1
ORCID: ORCID
Man-Sik Kong
1
ORCID: ORCID
Changhee Lee
2

  1. Advanced Materials & Processing Center, Institute for Advanced Engineering, Yongin, South Korea
  2. Hanyang University, Division of Materials Science and Engineering, Seoul, South Korea
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Abstract

Tungsten diselenide (WSe2) is one of the promising transition metal dichalcogenides (TMDs) for nanoelectronics and optoelectronics. To enhance and tune the electronic performance of TMDs, chemical functionalization via covalent and van der Waals approaches has been suggested. In the present report, the electric and structural transition of WSe2 oxidized by exposure to O3 is investigated using scanning tunneling microscopy. It is demonstrated that the exposure of WSe2/high-ordered pyrolytic graphite sample to O3 induces the formation of molecular adsorbates on the surface, which enables to increase in the density of states near the valence band edge, resulting from electric structural modification of domain boundaries via exposure of atomic O. According to the work function extracted by Kelvin probe force microscopy, monolayer WSe2 with the O3 exposure results in a gradual increase in work function as the exposure to O3. Therefore, the present report demonstrates the potential pathway for the chemical functionalization of TMDs to enhance the electric performance of TMDs devices.
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Authors and Affiliations

Eunjeong Kim
1
Sangyoeb Lee
2
ORCID: ORCID
Yeonjin Je
3
Dong Park Lee
3
Sang Jun Park
3
Sanghyun Jeong
2
Joon Sik Park
2
Byungmin Ahn
4
ORCID: ORCID
Jun Hong Park
1 3
ORCID: ORCID

  1. Gyeongsang National University, Department of Materials Engineering and Convergence Technology, Jinju, Korea
  2. Hanbat National University, Department of Materials Science and Engineering and Department of Materials and Manufacturing Engineering, Daejeon, Korea
  3. Gyeongsang National University, School of Materials Science and Engineering, Jinju, Korea
  4. Ajou University, Department of Materials Science and Engineering and Department of Energy Systems Research, Suwon, Korea
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Abstract

Increasing the operating temperature and pressure of an automotive engine and reducing its weight can improve fuel efficiency and lower carbon dioxide emissions. These can be achieved by changing the engine piston material from conventional aluminum alloy to high-strength heat- resistant steel. American Iron and Steel Institute 4140 modified steels (AISI 4140 Mod.s), which have improved strength, oxidation resistance, and wear resistance at high temperature were developed by adjusting the AISI 4140 alloy compositions and optimizing the heat treatment process for automotive engine applications. In this study, the effects of modifying alloy compositions on the microstructure, mechanical properties (both at room and high temperatures), and oxidation of AISI 4140 Mod.s were investigated. Effective grain refinement occurred due to the influence of high-temperature stable carbide forming elements such as Mo, and V. The bainite structure changed to martensite structure under the influence Cr and Ni. As the Cr and W contents increased, the oxidation resistance was improved, and the oxide layer thickness decreased after 10 hours exposure at 500°C. The AISI 4140 Mod. exhibited a 35% improvement in room temperature strength, 70% improvement in high-temperature strength, and 40% improvement in high-temperature oxidation resistance compared to conventional AISI 4140.
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Authors and Affiliations

Hyo-Seong Kim
1 2 3
ORCID: ORCID
Moonseok Kang
1
ORCID: ORCID
Minha Park
1
ORCID: ORCID
Byung Jun Kim
1
ORCID: ORCID
Byoungkoo Kim
1
ORCID: ORCID
Yong-Sik Ahn
2
ORCID: ORCID

  1. Korea Institute of Industrial Technology, 46938, Busan, Republic of Korea
  2. Pukyong National University, Department of Materials Science and Engineering, 48547, Busan, Republic of Korea
  3. HD Korea Shipbuilding & Offshore Engineering, 44032, Ulsan, Republic of Korea
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Abstract

This study investigated the effect of heat treatment on the microstructure and impact toughness property of AISI D2 manufactured with direct energy deposition (DED) and compared the results with conventional wrought material. The fracture crack propagation behavior was examined in connection with microstructures through fracture surface analysis. AISI D2 manufactured with DED had a eutectic structure that turned into a net-type carbide after heat treatment, and Cr-rich needle-type secondary carbide was observed. Impact toughness of DED AISI D2 measured 2.0 J/cm2 in the as-built sample and 1.1 J/cm2 in the heat-treated sample. Compared to a wrought heat-treated AISI D2, DED AISI D2 had relatively low impact toughness. DED AISI D2 and wrought material had different crack propagation mechanisms. In DED AISI D2, the eutectic structure and net-type carbide boundary were identified as the major microstructural factor decreasing impact toughness.
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Authors and Affiliations

Jung-Hyun Park
1
ORCID: ORCID
Kyu-Sik Kim
1
ORCID: ORCID
Yong-Mo Koo
2
ORCID: ORCID
Jin-Young Kim
3
ORCID: ORCID
Min-Chul Kim
4
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon 22212, Korea
  2. Changsung Corp., Incheon, 21628, Korea
  3. Maxrotech Corp., Daegu, 42703, Korea
  4. Korea Atomic Energy Research Institute (KAERI), Daejeon 34057, Korea
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Abstract

An open-cell Ni-Mo-Cr foam was newly manufactured using electrostatic powder spraying process and its room-temperature compressive properties were investigated in this study. For manufacturing Ni-Mo-Cr foam, Ni-Mo-Cr powders were sprayed on the polyurethane pre-form by electrostatic powder spraying process. And then, Ni-Mo-Cr powder sprayed pre-forms were sintered at 1200℃, 1250℃, and 1300℃, respectively. The relative densities of Ni-Mo-Cr foams were measured at 4 ~ 5%. Room temperature compressive curves of ESP Ni-Mo-Cr foams represented the typical compressive 3-stages (elastic, plateau, densification) of open-cell metallic foam. As a result of observation of deformed specimen, the fracture mode found to be changed from brittle to ductile as sintering temperature increased. Based on these findings, correlations between structural characteristics, microstructure, and compressive deformation behavior were also discussed.

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Authors and Affiliations

Tae-Hoon Kang
Kyu-Sik Kim
ORCID: ORCID
Min-Jeong Lee
ORCID: ORCID
Jung-Yeul Yun
ORCID: ORCID
Kee-Ahn Lee
ORCID: ORCID
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Abstract

In this study, the effect of rolling of 1.25Cr-1Mo-0.5V-0.3C American Iron and Steel Institute 4340 modified steel for highspeed railway brake discs on the microstructure and mechanical properties was investigated. The materials were hot-rolled at 0%, 51%, and 66% reduction ratios, and then analyzed by optical microscopy, scanning electron microscopy, and electron backscattering diffraction (EBSD). needle-shaped ferrite block morphology in bainite varied with the rolling ratio. EBSD analysis reveals dynamic recovery and dynamic recrystallization, affected ferrite block boundaries and dislocation densities during rolling. Mechanical tests showed that hardness, toughness and elongation increase at higher rolling reduction ratio, while strength remained relatively constant. In particular, the impact toughness increased almost twice from the level of 70 J in S1 (0% reduction) to the level of 130 J in S3 (66% reduction). These results showed that the hot rolling can significantly improve the strength and toughness combination of cast brake discs material.
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Authors and Affiliations

Hyo-Seong Kim
1 2 4
ORCID: ORCID
Moonseok Kang
1
ORCID: ORCID
Minha Park
1
ORCID: ORCID
Byung Jun Kim
1
ORCID: ORCID
Yong-Shin Kim
3
Tae Young Lee
3
Byoungkoo Kim
1
ORCID: ORCID
Yong-Sik Ahn
2
ORCID: ORCID

  1. Korea Institute of Industrial Technology, 46938, Busan, Republic of Korea
  2. Pukyong National University, Department of Materials Science and Engineering, 48547, Busan, Republic of Korea
  3. KATEM, 51395, Changwon, Republic of Korea
  4. HD Korea Shipbuilding & Offshore Engineering, 44032, Ulsan, Republic of Korea
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Abstract

Fractography of stress corrosion cracking (SCC) of 20% cold worked Type 304 H stainless steel containing δ-ferrite was studied using a compact tension (CT) specimen in oxidizing primary water with a scanning electron microscope (SEM) and electron back scattered diffraction (EBSD). The stress corrosion crack propagated mostly in transgranular stress corrosion cracking (TGSCC) mode and sometimes in intergranular stress corrosion cracking (IGSCC) mode. TGSCC paths were along the {111} plane with both high resolved shear stress and high resolved tensile stress. IGSCC preferentially propagated along the grain boundary perpendicular to the loading axis. The findings in this work suggest that TGSCC proceeds through formation of a weakening zone at the head of the crack tip by interaction of slip and corrosion and then cracking of the weakened zone by tensile stress.
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Authors and Affiliations

Hong-Pyo Kim
1
ORCID: ORCID
Jong-Yeon Lee
1
ORCID: ORCID
Sung-Hwan Cho
1
ORCID: ORCID
Min-Jae Choi
1
ORCID: ORCID
Sung-Woo Kim
1
ORCID: ORCID
Hyung-Ha Jin
1
ORCID: ORCID
Dong-Jin Kim
1
ORCID: ORCID
Seoung-Sik Hwang
1
ORCID: ORCID
Yun-Soo Lim
1
ORCID: ORCID

  1. Korea Atomic Energy Rese arch Institute , Materials Safety Research Division, 989-111 Daedeok-daero, Yuseong-gu, Daejeon, 305-353, Republic of Korea

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