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Abstrakt

The paper discusses experimental studies to determine the effect of the die working portion angle on the lubrication conditions, zinc coating thickness and the mechanical properties of medium-carbon steel wires. The test material was 5.5 mm-diameter wire rod which was drawn into 2.2 mm-diameter wire in seven draws at a drawing speed of v = 10 m/s. Conventional drawing dies of a working portion angle of α = 3, 4, 5, 6, 7°, respectively, were used for the drawing process. After the drawing process, the quantity of the lubricant on the wire surface and the thickness of the zinc coating were determined in individual draws. Testing the finished 2.2 mm-diameter wires for mechanical properties, on the other hand, determined the effect of the die working portion on the yield point, tensile strength, uniform and total elongation, reduction in area, the number of twists and the number of bends.

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Autorzy i Afiliacje

M. Suliga
R. Wartacz

Abstrakt

The paper discusses a theoretical and an experimental analyses of steel wire drawing in conical drawing dies with a varying length of the die sizing portion. The theoretical analysis was performed in the Drawing 2D, where the wire temperature and drawing stress were determined. The theoretical study was verified by the measurement of drawing force under laboratory conditions and by industrial multi-stage drawing tests carried out under commercial conditions. A relationship has been shown to exist between die sizing portion length and wire temperature and drawing stress.

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Autorzy i Afiliacje

M. Suliga
M. Jabłońska

Abstrakt

In this paper, an attempt was made to explain the causes of surface delamination in high carbon steel wires during the torsion test. For end wires with 1.7 mm diameter drawn at speeds of 5, 10, 15, 20, 25 m/s, technological tests were carried out. Then the susceptibility of the wire to plastic strain was determined. The microstructure analysis complemented the research. Analysis of the fracture torsion test showed that the wires drawn at speeds exceeding 15 m/s are delamination, which disqualify it as a material for a rope and a spring. The source of delamination in high carbon steel wires is their stronger strengthening, especially of the surface layer, which leads to a decrease in the orientation of the cementite laminaes and an increase in the degree of their fragmentation.

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Autorzy i Afiliacje

M. Suliga

Abstrakt

The paper analyzes the effect of ageing on the variations in the mechanical and technological properties of steel wire. The process of drawing 5.5 mm-diameter wire rod into 1.70 mm wire was carried out in 12 draws on a Koch KGT multi-stage drawing machine in the drawing velocity range of 5-25 m/s. Finished 1.7 mm-diameter wires after, respectively, 1, 24, 720 and 8760 hours of the completion of the drawing process were subjected to testing to determine their mechanical and technological properties. The yield strength, YS; tensile strength, UTS; uniform elongation, Ar; total elongation, Ac; reduction of area, Z; number of twists, Nt; and the number of bends, Nb, have been determined. It has been demonstrated that variations in mechanical properties occur after the multi-stage drawing process due to ageing, with their degree and mode being dependent on the drawing speed.

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Autorzy i Afiliacje

M. Suliga

Abstrakt

The state of the dislocation substructure of meteorite in which the history of phenomena accompanying the meteorite during its passage through the Earth’s atmosphere is recorded remains unused. The main goal of the presented work is a comprehensive analysis of the dislocation structure of the iron meteorite from the Morasko reserve (Poland, Wielkopolska Voivodeship) by TEM methods to determine the conditions and mechanism of its formation. The work is cognitive in the field of phenomena related to the destruction and deformation of the material in extreme conditions: space and terrestrial space. It can also be useful in the research on the creation of the material with specific mechanical properties, as well as a unique reference material for earth experiments with low-temperature deformation, high-speed deformation, recrystallization processes with short thermal pulses and structure relaxation in conditions of very long time periods.

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Autorzy i Afiliacje

W. Osuch
R. Błoniarz
G. Michta
I. Suliga

Abstrakt

An analysis of the effect of drawing speed on the formation of a zinc coating in the multi-stage fine steel wire drawing process has been carried out in the article. Pre-hardened 2.2 mm-diameter material was drawn into 1.00 mm-diameter wire in 6 draws on a multi-stage drawing machine. The drawing process was carried out at a drawing speed of 5, 10, 15, 20 and 20 m/s, respectively. Mechanical tests were tests were performed for the final wires to determine their yield strength, ultimate tensile strength, uniform and total elongation and reduction in area. The thickness of the zinc coating on the wire surface was determined by the gravimetric method and based on metallographic examination. The use of electron scanning microscopy, on the other hand, enabled the identification of individual phases in the zinc coating. The above investigations were supplemented with corrosion testing of 1.00 mm-diameter wires. It has been demonstrated that drawing speed significantly influences not only the thickness of the zinc coating on the drawn wire surface, buts also its morphology and corrosion resistance.

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Autorzy i Afiliacje

M. Suliga
R. Wartacz
H. Kania

Abstrakt

Powdered polyaniline (PANI) was synthesised chemically with different doping anions namely hydrochloric acid, sulphuric acid and para-toluenesulfonic acid (pTSA). Two-step synthetic procedure was utilised at low temperature. The highest reaction efficiency was found for chlorine-doped PANI. Structural characterization with FTIR revealed the vibration bands characteristic to formation of the emeraldine salt. The surface morphology of doped PANIs was studied by SEM images which showed near globular shape and porous structures with different size of the aggregated particles. They were smaller for Cl–- or pTS–-doped PANI while for SO42– the size was markedly larger. The XRD patterns revealed that there are ordered regions especially for pTS– doped PANI, while the highest conductivity value was recorded for Cl– doped one followed by organic pTS– doped and SO42– doped one.

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Autorzy i Afiliacje

S. Golba
M. Popczyk
S. Miga
J. Jurek-Suliga
M. Zubek

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